露兜簕茎皮化学成分研究

金燕,孙洋,吴悠楠,张彩云

中国药学杂志 ›› 2017, Vol. 52 ›› Issue (14) : 1223-1226.

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中国药学杂志 ›› 2017, Vol. 52 ›› Issue (14) : 1223-1226. DOI: 10.11669/cpj.2017.14.006
论著

露兜簕茎皮化学成分研究

  • 金燕,孙洋,吴悠楠,张彩云*
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Chemical Constituents from Stem Barks of Pandanus tectorius

  • JIN Yan, SUN Yang, WU You-nan, ZHANG Cai-yun*
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摘要

目的 研究露兜簕(Pandanus tectorius Soland.)茎皮的化学成分。方法 采用硅胶柱色谱、Sephadex LH-20 柱色谱、高效液相色谱分离化合物,通过理化数据测定和波谱技术分析确定所得化合物的结构。结果 从露兜簕茎皮乙醇提取物中分离得到10个化合物,分别鉴定为:1′-O-benzyl-α-L-rhamnopyranosyl-(1″→6′)-β-D-glucopyranoside (1), dihydrodehydrodiconiferyl alcohol (2),异牡荆素(3),牡荆素(4),3,5-二咖啡酰奎宁酸甲酯(5),3,5-二咖啡酰奎宁酸乙酯(6),3,4-二咖啡酰奎宁酸甲酯(7),(+)-lyoniresinol 3a-O-β-glucopyranoside(8),(-)-lyoniresinol 3a-O-β-glucopyranoside(9)和苄醇-β-D-吡喃葡萄糖苷(10)。结论 所有化合物均为首次从该植物中分离得到。

Abstract

OBJECTIVE To study the chemical constituents in the stem barks of Pandanus tectorius Soland. METHODS The compounds were isolated by repeated chromatography. Their structures were elucidated by spectroscopic methods. RESULTS Ten compounds were isolated and identified as 1′-O-benzyl-α-L-rhamnopyranosyl-(1″→6′)-β-D-glucopyranoside(1), dihydrodehydrodiconiferyl alcohol(2), isovitexin(3), vitexin(4), 3,5-di-O-caffeoylquinic acid methyl ester(5), 3,5-di-O-caffeoylquinic acid ethyl ester(6), 3,4-di-O-caffeoylquinic acid methyl ester(7),(+)-lyoniresinol 3a-O-β-glucopyranoside(8),(-)-lyoniresinol 3a-O-β-glucopyranoside(9), and benzyl-β-D-glucopyranoside(10). CONCLUSION All compounds are isolated from this plant for the first time.

关键词

露兜簕 / 茎皮 / 异牡荆素 / 牡荆素 / 3 / 5-二咖啡酰奎宁酸甲酯 / 3 / 5-二咖啡酰奎宁酸乙酯

Key words

Pandanus tectorius / stem bark / isovitexin / vitexin / 3,5-di-O-caffeoylquinic acid methyl ester / 3,5-di-O-caffeoylquinic acid ethyl ester

引用本文

导出引用
金燕,孙洋,吴悠楠,张彩云. 露兜簕茎皮化学成分研究[J]. 中国药学杂志, 2017, 52(14): 1223-1226 https://doi.org/10.11669/cpj.2017.14.006
JIN Yan, SUN Yang, WU You-nan, ZHANG Cai-yun. Chemical Constituents from Stem Barks of Pandanus tectorius[J]. Chinese Pharmaceutical Journal, 2017, 52(14): 1223-1226 https://doi.org/10.11669/cpj.2017.14.006
中图分类号: R284   

参考文献

[1] AN N, ZHANG T T, GUI M, et al.Chemical constituents from the stem bark of Pandanus tectorius . Chin Pharm J(中国药学杂志), 2015, 50(11): 931-934.
[2] WANG F Q, ZHANG J W, YAO G M, et al. Chemical constituents of Sapium sebiferum leaves . Chin Pharm J(中国药学杂志), 2013, 48(22): 1908-1911.
[3] OU Y F, LIU Y, LI R, et al. Five lignans and one iridoid from Sambucus williamsii . Chin J Nat Med(中国天然药物), 2011, 9(1): 26-29.
[4] YUAN L, HUANG W Z, LIANG D Q, et al. Study on flavonoid glycosides from the herb of Clematis connate . Chin Pharm J (中国药学杂志), 2015, 50(6): 497-501.
[5] LI S H. Chemical constituents of whole plant of Oxalis pes-caprae L. . Chin Pharm J (中国药学杂志), 2013, 48(21): 1820-1822.
[6] LIU Y F, YANG X W, WU B. Studies on chemical constituents in the buds of Tussilago farfara . China J Chin Mater Med(中国中药杂志), 2007, 32(22): 2378-2381.
[7] GONG S S, LIU Y L, LI Y, et al. Chemical constituents from whole plant of Gynura procumbens(I) . Chin Tradit Herb Drugs (中草药), 2016, 47(11): 1856-1860.
[8] CHANG X L, LI J, WU L J, et al. Chemical constituents from aerial parts of Argyreia seguinii . Chin Tradit Herb Drugs (中草药), 2006, 37(2): 178-181.
[9] ACHENBACH H, LOWEL M, WAIBEL R, et al. New lignan glucosides from Stemmadenia minima . Planta Medica, 1992, 58(3): 270-272.
WANG F, JIANG Y L, WANG X L, et al. Chemical constituents from flower buds of Lonicera japonica . China J Chin Mater Med(中国中药杂志), 2013, 38(9): 1378-1385.

基金

国家自然科学基金资助项目(81202994)
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